Rat interleukin 5 (IL-5) enzyme-linked technology

**Rat Interleukin 5 (IL-5) Enzyme-Linked Immunosorbent Assay (ELISA) Kit Instruction Manual** This reagent is intended for research purposes only and not for human diagnostic use. The kit is designed to quantitatively measure the levels of Interleukin-5 (IL-5) in various biological samples, including rat serum, plasma, cell culture supernatants, and other similar liquid specimens. **Principle of the Assay** The IL-5 ELISA kit utilizes a sandwich immunoassay method. A microtiter plate is pre-coated with a specific monoclonal antibody against rat IL-5. After incubation with the sample, the IL-5 present in the sample binds to the immobilized antibody. A second biotinylated detection antibody is then added, followed by horseradish peroxidase (HRP)-conjugated streptavidin. The enzyme-substrate reaction leads to color development, which is proportional to the concentration of IL-5 in the sample. The optical density (OD) is measured at 450 nm using a microplate reader, and the concentration is determined by comparing the OD values to a standard curve. **Kit Components** - Microtiter Plate: 1×48 or 1×96 wells - Standard: 0.5 ml × 1 vial (1350 pg/ml) - Standard Diluent: 1.5 ml × 1 vial - Enzyme Conjugate: 3 ml × 1 vial - TMB Substrate: 3 ml × 1 vial - Stop Solution: 3 ml × 1 vial - Wash Buffer (20×): 20 ml × 20 times or 20 ml × 30 times - Sealing Film: 2 pieces - Storage: 2–8°C **Sample Preparation and Handling** Proper sample handling is crucial for accurate results. - **Serum**: Allow blood to clot at room temperature for 10–20 minutes, then centrifuge at 2000–3000 rpm for 20 minutes. - **Plasma**: Use EDTA or sodium citrate as anticoagulant, mix well, and centrifuge similarly. - **Urine**: Collect in a sterile container and centrifuge. - **Cell Culture Supernatant**: Centrifuge after collection. For intracellular components, lyse cells via repeated freeze-thaw cycles before centrifugation. - **Tissue Homogenate**: Weigh the tissue, homogenize in PBS, and centrifuge. Store remaining samples at –20°C if not used immediately. **Assay Procedure** 1. **Standard Dilution**: Prepare serial dilutions of the IL-5 standard on the microtiter plate. 2. **Sample Addition**: Add 40 μl of sample diluent and 10 μl of sample to each well. 3. **Incubation**: Seal the plate and incubate at 37°C for 30 minutes. 4. **Washing**: Wash the plate five times with wash buffer. 5. **Enzyme Conjugate**: Add 50 μl of HRP-labeled antibody to each well. 6. **Second Incubation**: Incubate again at 37°C for 30 minutes. 7. **Color Development**: Add 50 μl of TMB A and B solutions, incubate for 15 minutes. 8. **Stop Reaction**: Add 50 μl of stop solution to each well. 9. **Reading**: Measure OD at 450 nm within 15 minutes of stopping the reaction. **Notes and Recommendations** - Allow the kit to equilibrate to room temperature before use. - Avoid cross-contamination by using a new sealing film for each experiment. - Ensure all reagents are properly mixed and handled. - Always prepare a standard curve and run samples in duplicate. - If sample OD exceeds the highest standard, perform a dilution before testing. - Do not use NaN3-containing samples, as it may inhibit HRP activity. - All waste should be treated as biohazardous material. **Data Analysis** Plot the standard curve using the OD values vs. IL-5 concentrations. Calculate the sample concentration using linear regression or by interpolating from the standard curve. Multiply the result by the dilution factor if applicable. **Performance Characteristics** - Sensitivity: 1 pg/ml - Dynamic Range: 1 pg/ml – 1000 pg/ml - Intra-assay CV < 9%, Inter-assay CV < 11% - Correlation coefficient (R²) > 0.95 **Storage and Shelf Life** - Store the kit at 2–8°C. - Shelf life: 6 months from the date of manufacture. This manual provides detailed instructions for the accurate and reliable measurement of IL-5 in rat samples. Following these guidelines ensures consistent and reproducible results.

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